X-ray powder diffraction beamline at D10B of LNLS: application to the Ba2FeReO6 double perovskite

Ferreira, F.F.; Granado, E.; Carvalho, W. Jr; Kycia, S.W.; Bruno, D.; Droppa, R. Jr

doi:10.1107/S0909049505039208

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Figure 7
Observed (cross symbols) and calculated (solid line) high-resolution X-ray powder diffraction intensities in a selected angular interval for Ba₂FeReO₆ at (a) 14 K with the Rietveld refinement performed under a tetragonal model (space group I4/mmm), and (b) 400 K with the refinement under a cubic model (space group Pm $[\bar3]$ m). The difference profiles are also given. Short vertical bars correspond to the calculated Bragg peak positions. The wavelength was λ = 1.37728 Å. The total collection time for each profile (15° ≤ 2θ ≤ 150°) was ∼4 h.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 13| Part 1| December 2006| Pages 46-53

https://doi.org/10.1107/S0909049505039208

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