A versatile in situ spectroscopic cell for fluorescence/transmission EXAFS and X-ray diffraction of heterogeneous catalysts in gas and liquid phase

Hannemann, S.; Casapu, M.; Grunwaldt, J.-D.; Haider, P.; Trüssel, P.; Baiker, A.; Welter, E.

doi:10.1107/S0909049507024466

Journal of Synchrotron Radiation Journal of
Synchrotron Radiation

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Figure 2
Schematic view of the heatable/coolable in situ fluorescence/transmission EXAFS cell also suited to X-ray diffraction. A and A1: gas inlet for the reaction mixture; B and B1: gas outlet of the product gas towards gas analysis; C: reaction cell of stainless steel; H: heat plate with Thermocoax heater and liquid-nitrogen cooling; I: inset; M: main body with Kapton windows (W) and sealings (R) and an outlet to the vacuum pump (V); P1 and P2: plates to assemble the in situ cell; S2 and S3: sealing for the in situ cell; T1 and T2: thermocouples [a Teflon ring (TR) is optionally used, see text].

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 14| Part 4| July 2007| Pages 345-354

https://doi.org/10.1107/S0909049507024466

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