Figure 3
The sample holder H and reaction cell C with the path of the X-ray beam: (a) three-dimensional schematics from the top; (b) cross section through the centre of the in situ cell (the angles show the opening angle of the plate P2 and the heater H, which are required for the fluorescence XAS and the powder diffraction data); notation like in Fig. 2; in addition, the screws (Sc1 to Sc3) to mount the cell are depicted. |