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Figure 6
Combined Mo K-edge XANES (a) with combined temperature/time profile (b), raw SAXS data (c) with analysis of gradient versus time (d), WAXS (e) and mass spectrometry data (f) recorded during the heating of a FeMo catalyst under MeOH/He and in air conditions. Feature B in (a) highlights the 1s–4d peak at the Mo K-edge.

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