Implementation of a combined SAXS/WAXS/QEXAFS set-up for time-resolved in situ experiments

Nikitenko, S.; Beale, A.M.; van der Eerden, A.M.J.; Jacques, S.D.M.; Leynaud, O.; O'Brien, M.G.; Detollenaere, D.; Kaptein, R.; Weckhuysen, B.M.; Bras, W.

doi:10.1107/S0909049508023327

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Figure 6
Combined Mo K-edge XANES (a) with combined temperature/time profile (b), raw SAXS data (c) with analysis of gradient versus time (d), WAXS (e) and mass spectrometry data (f) recorded during the heating of a FeMo catalyst under MeOH/He and in air conditions. Feature B in (a) highlights the 1s–4d peak at the Mo K-edge.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 15| Part 6| October 2008| Pages 632-640

doi:10.1107/S0909049508023327

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