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Figure 2
Calorimetric scan of the melting of a pure Sn reference sample with and without the X-ray beam, which was set to 11.1 keV, where the absorption by Sn is high. The small shift in the baseline might originate from the X-ray absorption or from a repositioning of the sample. The resulting temperatures and enthalpies are reliable in both cases, since they are unaffected by the X-rays and are in good agreement with literature values.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 19| Part 5| July 2012| Pages 806-813
doi:10.1107/S090904951202612X
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