Figure 7
Variation in size of particles over the Guinier and fringed regions at each temperature. For each temperature the Guinier data are represented by a filled triangle, the elliptical a-axis by an open square, the elliptical b-axis by a cross, and the elliptical c-axis by an open circle. All data have been plotted only while the axial-length values remain within the available SAXS q-scale. For clarity not all data points are included: at 333 K, in the Guinier region, data are plotted every 5 min, and in the fringed region, every 10 min; at 353 K, all datasets are present except for the elliptical a-axis within the fringed region, where datasets are presented every 1.5 min; at 368 K, in the Guinier region, data are presented every 0.25 min, while in the fringed region the elliptical a-axis is presented every 0.5 min, and all data are shown for the other axes. Fitting errors are comparable with the size of the data point. |