Design and development of a controlled pressure/temperature set-up for in situ studies of solid–gas processes and reactions in a synchrotron X-ray powder diffraction station

Salas-Colera, E.; Muñoz-Noval, Á.; Heyman, C.; Ania, C.O.; Parra, J.B.; García-Granda, S.; Calero, S.; Rubio-Zuazo, J.; Castro, G.R.

doi:10.1107/S1600577514021018

Journal of Synchrotron Radiation Journal of
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Figure 2
(a) Scheme of the rotation sample holder. The three main elements of this device are pointed out: on the left the rotor system, in the middle the flexible house, and on the right the rotary union. (b) Scheme of the shaft rotor. For clarity the expanded/dismount part are presented: top, shaft-rotor; bottom, capillary support sample holder pipe. The different components are shown (see text). (c) Scheme of the rotary union. The different components are shown (see text).

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 22| Part 1| January 2015| Pages 42-48

https://doi.org/10.1107/S1600577514021018

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