Design and development of a controlled pressure/temperature set-up for in situ studies of solid–gas processes and reactions in a synchrotron X-ray powder diffraction station

Salas-Colera, E.; Muñoz-Noval, Á.; Heyman, C.; Ania, C.O.; Parra, J.B.; García-Granda, S.; Calero, S.; Rubio-Zuazo, J.; Castro, G.R.

doi:10.1107/S1600577514021018

Journal of Synchrotron Radiation Journal of
Synchrotron Radiation

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Figure 5
(a) N₂ ZIF-8 isothermal gas adsorption experiments carried out at 85 K and different N₂ pressures. The inset shows details of the region in which one of the most characteristic peaks of the adsorption process appears. The numbers in the diffraction data correspond to the sequence of gas dosing in the adsorption branch. (b) Ar ZIF-8 isothermal gas adsorption experiments carried out at 85 K and different Ar pressures. The inset shows four examples of details of the regions in which the used peaks of the adsorption process appear. The numbers in the diffraction data correspond to the sequence of gas dosing in the adsorption branch.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 22| Part 1| January 2015| Pages 42-48

https://doi.org/10.1107/S1600577514021018

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