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Figure 2
Background-subtracted PXRD patterns for all as-prepared and annealed Ca1 (a–c) and Cs1 (d–f) samples; reference for diamond-type Ge (JCPDS No. 4-545) is shown as blue marks at the bottom. `Hex' in the sample name means a suspension in hexane, and `Eth' for ethanol; `Ar' means synthesis with Ar gas protection and `H2Ar' for a mixture of H2 and Ar. The background was subtracted using PXRD measurement of an empty capillary. The inset image is SEM for Ca1 annealed 600.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 22| Part 1| January 2015| Pages 105-112
https://doi.org/10.1107/S1600577514022486
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