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Figure 1
XANES spectra of staurolite and pre-edge extraction models for HERFD-XANES data recorded in 0.05 eV increments (a) and high-resolution transmission-mode XANES data recorded in 0.25 eV increments (c). The functions for modelling the edge onset, i.e. the inclined arctangent, arctangent, two Gaussian functions and cubic spline, are displayed with the XANES spectra they are applied to. The resulting extracted pre-edge peaks are shown offset for clarity. The fitting residuals are magnified by a factor of 100 (HERFD) and 10 (high-resolution transmission) to show the misfit and the standard deviation (σ) is given. Details in the pre-edge region of plots (a) and (c) are shown in plots (b) and (d), respectively.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 22| Part 2| February 2015| Pages 410-426
doi:10.1107/S1600577514025880
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