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Figure 3
(a) Experimental setup for the in situ X-ray diffraction studies on the powder diffraction beamline at the Australian Synchrotron, and (b) the electrochemical flow cell. (A) Mythen detector; (B) electrolyte reservoir; (C) peristaltic pump; (D) flow cell; (E) XYZ stage; (F) spill tray; (G) working electrode lead; (H) reference electrode lead; (I) counter electrode lead; (J) Pb substrate; (K) electrolyte inlet; (L) electrolyte outlet.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 22| Part 2| January 2015| Pages 366-375
doi:10.1107/S1600577514027659
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