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Figure 2
(a) The C.Esp1396I crystal within the rayon fibre loop during data collection. Crystal dimensions were x = 30 µm and y = 30 µm. The crystal is positioned in the loop such that dimension z = 10 µm is directly into the page. The blue box shown around the crystal is 50 µm × 50 µm. A faint purple ring, formed by the production of solvated electrons, can be seen to the left of the crystal. This was created from a test shot of the X-ray beam prior to crystal centring and confirms the circular 25 µm beam profile generated from the pinhole. (b, c) RADDOSE-3D (Zeldin et al., 2013bBB49) calculation of dose distributions in the triangular C.Esp1396I crystal after (b) the first dataset and (c) the eighth dataset. In (b) the dose isosurfaces represent 0.16 MGy (white), 3.3 MGy (brown) and 4.2 MGy (orange) and in (c) 0.16 MGy (white), 20 MGy (blue) and 47.5 MGy (dark red). The direction of the X-ray beam is indicated with an arrow and the crystal was rotated about a horizontal axis.

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