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Figure 7
Fe K-edge XANES of an Rh–Fe/Ca–Al2O3 catalyst reduced under flowing H2. The catalyst was reduced in 10% H2 mixed with He at three different temperatures, 550, 650 and 700 K, with a heating rate of 10 K min−1. The temperature was held for one hour at each temperature mentioned above. Five XANES spectra were selected from hundreds of data sets to follow the reducibility of this catalyst.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
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