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Figure 2
A three-chambered cryostat cell is filled with three solutions [15 mM, 1.5 mM nickel(II) complex and pure solvent]. A precise flow of solution into the chambers was achieved using three 10 ml syringe pumps, with fittings, and 1/16′′ Teflon tubes. The cell, mounted on a cryostat stick, was clamped in the horizontal plane. Each syringe pump was controlled by a stepper-motor controller programmed by software to pulse the syringe pumps.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 22| Part 4| July 2015| Pages 1008-1021
https://doi.org/10.1107/S1600577515006190
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