Figure 1
As K-edge XANES spectra of (a) unaerated As(III)-reacted FeS at pH 9 using a He flow sample chamber, (b) unaerated As(III)-reacted FeS at pH 9 without exclusion of the atmospheric O2, (c) a mixture of the thoroughly aerated FeS and As2S3 using a He flow sample chamber, and (d) a mixture of the thoroughly aerated FeS and As2S3 without exclusion of the atmospheric O2. The beam exposure time was about 37 min per scan in a series of multiple scans. |