In situ observation of phase changes of a silica-supported cobalt catalyst for the Fischer–Tropsch process by the development of a synchrotron-compatible in situ/operando powder X-ray diffraction cell

Hoffman, A.S.; Singh, J.A.; Bent, S.F.; Bare, S.R.

doi:10.1107/S1600577518013942

Journal of Synchrotron Radiation Journal of
Synchrotron Radiation

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Figure 1
In situ capillary cell design for the characterization of powder samples in flowing atmospheres at elevated temperatures and pressures. (Top) Up-beam side of cell. (Bottom) Top-down showing flow path. The green arrow indicates movement of the outlet block to accommodate variable-length capillaries.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 25| Part 6| November 2018| Pages 1673-1682

https://doi.org/10.1107/S1600577518013942

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