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Figure 4
Diffraction patterns collected during the temperature-programmed reduction from 298 to 723 K of the Co/silica gel catalyst in flowing H2 (left), and select diffraction patterns as a function of temperature during the reduction (right) with reference patterns of Co3O4 (black), CoO (red) and f.c.c. Co (blue) displayed below. Inset: close-up of the top of the diffraction peak near 2.59 Å−1 highlighting the shift in peak position as a function of temperature.

Journal logoJOURNAL OF
SYNCHROTRON
RADIATION
ISSN: 1600-5775
Volume 25| Part 6| November 2018| Pages 1673-1682
https://doi.org/10.1107/S1600577518013942
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