In situ observation of phase changes of a silica-supported cobalt catalyst for the Fischer–Tropsch process by the development of a synchrotron-compatible in situ/operando powder X-ray diffraction cell

Hoffman, A.S.; Singh, J.A.; Bent, S.F.; Bare, S.R.

doi:10.1107/S1600577518013942

Journal of Synchrotron Radiation Journal of
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Figure 5
Diffraction patterns collected during the carburization of the reduced Co/silica gel catalyst in 20 bar CO at 523 K as a function of time since hydrogen was removed from the gas stream (left) and diffraction patterns at 0 and 340 min, prior to and post carburization (right) with reference patterns of CoO (black), f.c.c. Co (red) and Co₂C (blue) displayed below.

JOURNAL OF
SYNCHROTRON
RADIATION

ISSN: 1600-5775

Volume 25| Part 6| November 2018| Pages 1673-1682

https://doi.org/10.1107/S1600577518013942

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