Stoichiometry-dependent structures: an X-ray and neutron single-crystal diffraction study of the effect of reaction stoichiometry on the crystalline products formed in the potassium–cyanurate system

Nichol, G.S.; Clegg, W.; Gutmann, M.J.; Tooke, D.M.

doi:10.1107/S0108768106025171

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 8
Part of the correct structure of (3) determined by neutron diffraction. The pseudo-mirror symmetry of the structure is approximately observed by all atoms except D5 and D16B. Their positions break the symmetry and result in extra weak reflections in the diffraction pattern which were not identified by X-ray diffraction.

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 62| Part 5| September 2006| Pages 798-807

doi:10.1107/S0108768106025171

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