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Figure 12
The 2:1 adduct between 1,3-DMTU and dioxane. The hydrogen bond within the asymmetric unit is indicated by a dashed line. The dioxane molecule has been completed by symmetry; only the asymmetric unit is numbered. Selected molecular dimensions (Å, °): S1—C2 1.7110 (8), N1—C2 1.3386 (10), N1—C11 1.4541 (10), C2—N3 1.3389 (10), N3—C31 1.4571 (11), O1—C4 1.4283 (10), O1—C3 1.4335 (11), C2—N1—C11 124.91 (7), N1—C2—N3 117.26 (7), N1—C2—S1 119.96 (6), N3—C2—S1 122.79 (6), C2—N3—C31 125.38 (7), C4—O1—C3 110.26 (6).

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ISSN: 2052-5206
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