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Figure 8
Comparison of the Flack parameter (red) and its s.u. (green) for 28 data sets, determined as part of a full matrix refinement with all the other structural parameters versus the values obtained by refinement of a small block containing only the overall scale and the Flack parameters. The points lie on lines of unit gradient, indicating the full and block matrix refinements are essentially equivalent.

Journal logoSTRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS
ISSN: 2052-5206
Volume 72| Part 5| October 2016| Pages 661-683
https://doi.org/10.1107/S2052520616012890
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