view article

Figure 4
(a) Normalized forward scattering at T = 77 K versus CPA solution critical cooling rate (CCR) as determined from fits to the data in Fig. 2[link](c) and fits to the critical cooling rate (CCR) versus CPA concentration data (Warkentin et al., 2013BB53) shown in Supplementary Fig. S3, given by (5)[link] with parameters β given in Supplementary Table S1. The CPA concentrations corresponding to critical cooling rates of 1 K s−1 range from ∼36%(w/w) for ethanol to ∼57%(w/w) for ethylene glycol. Critical cooling rate versus concentration data are not available for 2-propanol, MPD and polypropylene glycol. (b) Volume contraction Δv/v = [v(77 K) − v(298 K)]/v(298 K) in % for rapid cooling from room temperature to the glassy/vitreous/amorphous phase versus the critical cooling rate of the CPA solution.

Journal logoSTRUCTURAL
BIOLOGY
ISSN: 2059-7983
Follow Acta Cryst. D
Sign up for e-alerts
Follow Acta Cryst. on Twitter
Follow us on facebook
Sign up for RSS feeds