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Figure 4
Geometry refinement against simulated data was performed assuming either typical electron diffraction geometry or X-ray diffraction geometry, as described in the text. Corrgrams were produced for the final step of refinement to provide immediate visual feedback regarding correlations between the effects of refined parameters on the model. The colours and areas of the circles are related to the values of the correlation coefficient, with large blue circles indicating strong correlation and large red circles indicating strong anticorrelation. This plot shows the correlation between the effects of different parameters on the angular residuals (φφo), with the refined detector parameters excluded from the plots as they have no effect on the φ residuals. The parameter labels are as defined in Waterman et al. (2016BB65). The upper panel shows the corrgram for the electron diffraction geometry and the lower panel shows the equivalent corrgram for the X-ray diffraction geometry.

Journal logoSTRUCTURAL
ISSN: 2059-7983
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