Acta Cryst. (2001). E57, m23-m24  [ doi:10.1107/S1600536800019486 ]

[TcCl(CS)(dppe)₂]·C₆H₆

J. C. Bryan, A. K. Burrell and G. J. Kubas

Key indicators

• Single-crystal X-ray study
• T = 203 K
• Mean (C-C) = 0.004 Å
• Disorder in main residue
• R factor = 0.032
• wR factor = 0.098
• Data-to-parameter ratio = 19.4

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           29.00                 
         From the CIF: _reflns_number_total               6069                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         6622                           
         Completeness (_total/calc)             91.65%                          
          Alert C: < 95% complete                                               

PLAT_301  Alert C Main residue disorder ........................       5.00 Perc.


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 2 Alert Level C = Please check

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