Acta Cryst. (2001). E57, o594-o595 [ doi:10.1107/S1600536801009710 ]
No syntax errors found ADDSYM reports no extra symmetry
Alert Level B:
PLAT_360 Alert B Short C(sp3)-C(sp3) Bond C(15) - C(16) = 1.32 Ang.
|Author response: As discussed in the Comment and exptl_refinement sections, the ethyl ester group is probably disordered, but the data quality does not permit a rational modelling of the disorder.|
REFLT_03 From the CIF: _diffrn_reflns_theta_max 25.00 From the CIF: _reflns_number_total 1588 Count of symmetry unique reflns 1590 Completeness (_total/calc) 99.87% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 0 Fraction of Friedel pairs measured 0.000 Are heavy atom types Z>Si present no Please check that the estimate of the number of Friedel pairs is correct. If it is not, please give the correct count in the _publ_section_exptl_refinement section of the submitted CIF.
0 Alert Level A = Potentially serious problem
1 Alert Level B = Potential problem
0 Alert Level C = Please check
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