Acta Cryst. (2001). E57, m451-m453  [ doi:10.1107/S1600536801014994 ]

Square [Pd₄(-CN)₄(C₆F₅)₄(PEt₃)₄]·2C₆H₅CH₃

J. P. H. Charmant, P. Espinet and K. Soulantica

Online 20 September 2001

Key indicators

• Single-crystal X-ray study
• T = 173 K
• Mean (C-C) = 0.004 Å
• Disorder in main residue
• R factor = 0.025
• wR factor = 0.061
• Data-to-parameter ratio = 19.4

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



ABSTM_02  Alert C The ratio of expected to reported Tmax/Tmin(RR') is < 0.90    
          Tmin and Tmax reported:      0.695     0.801                          
          Tmin' and Tmax expected:      0.710     0.717                         
          RR' =      0.876                                                      
          Please check that your absorption correction is appropriate.          

PLAT_301  Alert C Main Residue Disorder ........................       9.00 Perc.

General Notes



ABSTM_02  When printed, the submitted absorption T values will be replaced      
          by the scaled T values. Since the ratio of scaled T's is              
          identical to the ratio of reported T values, the scaling does         
          not imply a change to the absorption corrections used in the          
          study.                                                                
          Ratio of Tmax expected/reported      0.895                            
          Tmax scaled      0.717 Tmin scaled      0.622                         


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 2 Alert Level C = Please check

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