(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2001). E57, o1252-o1254 [ doi:10.1107/S1600536801020153 ]

Photochemical formation of 2-acetyl-7-methylbenz[e]indole

A. Visnjevac, N. Basaric, B. Kojic-Prodic and M. Sindler-Kulyk

Online 30 November 2001

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.005 Å
R factor = 0.056
wR factor = 0.168
Data-to-parameter ratio = 8.7

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           74.87                 
         From the CIF: _reflns_number_total               1398                  
         Count of symmetry unique reflns         1398                           
         Completeness (_total/calc)            100.00%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured         0                           
         Fraction of Friedel pairs measured     0.000                           
         Are heavy atom types Z>Si present           no                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.