Acta Cryst. (2002). E58, o473-o475  [ doi:10.1107/S1600536802005391 ]

A diphenylboron chelate of an ethylenebishydroxylamine formaldehyde adduct

W. Kliegel, H. Amt, B. O. Patrick, S. J. Rettig and J. Trotter

Online 5 April 2002

Key indicators

• Single-crystal X-ray study
• T = 294 K
• Mean (C-C) = 0.003 Å
• R factor = 0.038
• wR factor = 0.051
• Data-to-parameter ratio = 10.9

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           77.40                 
         From the CIF: _reflns_number_total               2975                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         3455                           
         Completeness (_total/calc)             86.11%                          
          Alert B: < 90% complete (theta max?)                                  


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 0 Alert Level C = Please check

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