(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, m471-m472 [ doi:10.1107/S1600536802014113 ]

Tris(propane-1,3-diamine)nickel(II) bis(tetrafluoroborate)

R. D. Willett and F. F. Awwadi

Online 16 August 2002

Key indicators

Single-crystal X-ray study
T = 298 K
Mean (C-C) = 0.011 Å
Disorder in solvent or counterion
R factor = 0.059
wR factor = 0.139
Data-to-parameter ratio = 11.3

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_302  Alert C Anion/Solvent Disorder .......................      44.00 Perc.

PLAT_420  Alert C D-H Without Acceptor       N(1)   -   H(1A)             ?

PLAT_420  Alert C D-H Without Acceptor       N(6)   -   H(6A)             ?

PLAT_420  Alert C D-H Without Acceptor       N(10)  -   H(10A)            ?

PLAT_420  Alert C D-H Without Acceptor       N(11)  -   H(11B)            ?

PLAT_420  Alert C D-H Without Acceptor       N(15)  -   H(15A)            ?

General Notes



ABSTM_02  When printed, the submitted absorption T values will be replaced      
          by the scaled T values. Since the ratio of scaled T's is              
          identical to the ratio of reported T values, the scaling does         
          not imply a change to the absorption corrections used in the          
          study.                                                                
          Ratio of Tmax expected/reported      1.093                            
          Tmax scaled      0.810 Tmin scaled      0.715                         


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 6 Alert Level C = Please check