(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, m519-m520 [ doi:10.1107/S1600536802015787 ]

Bis(-N-(3-[3-indenyl]propyl-p-toluenesulfamido-N,O,O')-dimethylamidodichorotitanium)

C. Lensink, G. J. Gainsford and M. J. R. Brandsma

Online 13 September 2002

Key indicators

Single-crystal X-ray study
T = 170 K
Mean (C-C) = 0.007 Å
R factor = 0.052
wR factor = 0.140
Data-to-parameter ratio = 17.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



ABSTM_02  Alert B The ratio of expected to reported Tmax/Tmin(RR') is < 0.75    
          Tmin and Tmax reported:      0.393     0.892                          
          Tmin' and Tmax expected:      0.771     0.892                         
          RR' =      0.510                                                      
          Please check that your absorption correction is appropriate.

Author response: The ratio given is that given in summary after the SADABS run; It seems possible that the smallest dimension is inaccurate, but the crystal is no longer available to be re-measured.


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 0 Alert Level C = Please check