(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, m756-m757 [ doi:10.1107/S1600536802021256 ]

Tris(N-butyl-N-ethyldithiocarbamato)bismuth(III)

I. Baba, K. Karimah, Y. Farina, A. H. Othman, A. R. Ibrahim, A. Usman, H.-K. Fun and S. W. Ng

Online 30 November 2002

Key indicators

Single-crystal X-ray study
T = 183 K
Mean (C-C) = 0.014 Å
R factor = 0.059
wR factor = 0.162
Data-to-parameter ratio = 25.7

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



ABSTM_02  Alert C The ratio of expected to reported Tmax/Tmin(RR) is > 1.10     
          Tmin and Tmax reported:      0.254     0.433                          
          Tmin and Tmax expected:      0.167     0.366                          
          RR =      1.288                                                       
          Please check that your absorption correction is appropriate.          

PLAT_213  Alert C Atom C6      has ADP max/min Ratio ...........       3.50 prolate

PLAT_702  Alert C Angle   Calc   136.16(5), Rep  136.10(10), Dev.      1.20 Sigma
                     S2   -BI1  -S6      1.555   1.555   1.555

PLAT_702  Alert C Angle   Calc   124.56(5), Rep  124.50(10), Dev.      1.20 Sigma
                     S1   -BI1  -S5      1.555   1.555   2.666

PLAT_731  Alert C Bond    Calc     1.51(3), Rep    1.509(9) ....       3.33 su-Ratio
                     C6   -C7      1.555   1.555

General Notes



ABSTM_02  When printed, the submitted absorption T values will be replaced      
          by the scaled T values. Since the ratio of scaled T's is              
          identical to the ratio of reported T values, the scaling does         
          not imply a change to the absorption corrections used in the          
          study.                                                                
          Ratio of Tmax expected/reported      0.846                            
          Tmax scaled      0.366 Tmin scaled      0.215                         


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 5 Alert Level C = Please check