Acta Cryst. (2003). E59, m142-m144  [ doi:10.1107/S1600536803004744 ]

Di--acetato-³O,O':O'-di--trichloroacetato-²O:O'-bis[aqua(trichloroacetato)(1,10-phenanthroline-²N,N')praseodymium(III)] dimethylformamide disolvate

S.-Y. Zhang, Z. Shi, Z. Long-Guan, R.-R. Xu and W.-Q. Pang

Online 7 March 2003

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.010 Å
• R factor = 0.031
• wR factor = 0.078
• Data-to-parameter ratio = 11.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



THETM_01  Alert B The value of sine(theta_max)/wavelength is less than 0.575    
          Calculated sin(theta_max)/wavelength =    0.5563                      

 Alert Level C:



PLAT_731  Alert C Bond    Calc     0.88(5), Rep     0.88(2) ....       2.50 su-Ratio
                     O1   -H1A     1.555   1.555

PLAT_731  Alert C Bond    Calc     0.89(6), Rep     0.89(2) ....       3.00 su-Ratio
                     O1   -H1B     1.555   1.555

PLAT_731  Alert C Bond    Calc     1.24(4), Rep   1.248(19) ....       2.11 su-Ratio
                     N3   -C21     1.555   1.555

PLAT_735  Alert C D-H     Calc     0.88(5), Rep     0.88(2) ....       2.50 su-Ratio
                     O1   -H1A     1.555   1.555

PLAT_735  Alert C D-H     Calc     0.89(6), Rep     0.89(2) ....       3.00 su-Ratio
                     O1   -H1B     1.555   1.555


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 5 Alert Level C = Please check

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