Acta Cryst. (2003). E59, m155-m156  [ doi:10.1107/S160053680300429X ]

cis-Dichlorobis(4,4'-dimethyl-2,2'-bipyridine)iridium(III) hexafluorophosphate

N. Yoshikawa, J. Sakamoto, N. Kanehisa, Y. Kai and T. Matsumura-Inoue

Online 14 March 2003

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.009 Å
• R factor = 0.053
• wR factor = 0.126
• Data-to-parameter ratio = 18.3

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     17
                   CL1 -IR1 -N1  -C1     93.00  3.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     18
                   CL1 -IR1 -N1  -C5    -79.00  3.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     29
                   CL2 -IR1 -N3  -C13   171.00  1.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     30
                   CL2 -IR1 -N3  -C17    -9.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     49
                   N2  -IR1 -N4  -C18   -63.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     50
                   N2  -IR1 -N4  -C22   118.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     70
                   N4  -IR1 -N2  -C6    -40.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     71
                   N4  -IR1 -N2  -C10   142.00  2.00   1.555   1.555   1.555   1.555


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 8 Alert Level C = Please check

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