Acta Cryst. (2003). E59, m273-m275  [ doi:10.1107/S1600536803008651 ]

Bis[1,2-bis(diphenylphosphino)ethane]silver(I) bis(trifluoroacetato)triphenylstannate(IV)

C. F. Chee, K. M. Lo and S. W. Ng

Online 30 April 2003

Key indicators

• Single-crystal X-ray study
• T = 168 K
• Mean (C-C) = 0.008 Å
• R factor = 0.042
• wR factor = 0.122
• Data-to-parameter ratio = 17.0

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



ABSTM_02  Alert C The ratio of expected to reported Tmax/Tmin(RR') is < 0.90    
          Tmin and Tmax reported:      0.518     0.742                          
          Tmin' and Tmax expected:      0.664     0.751                         
          RR' =      0.790                                                      
          Please check that your absorption correction is appropriate.          

PLAT_601  Alert C Structure Contains Solvent Accessible VOIDS of      70.00 A   3

PLAT_732  Alert C Angle   Calc    84.70(4), Rep   84.70(10) ....       2.50 su-Ratio
                     P1   -AG1  -P2      1.555   1.555   1.555

PLAT_732  Alert C Angle   Calc   124.30(4), Rep  124.30(10) ....       2.50 su-Ratio
                     P1   -AG1  -P3      1.555   1.555   1.555

PLAT_732  Alert C Angle   Calc   118.51(4), Rep  118.50(10) ....       2.50 su-Ratio
                     P1   -AG1  -P4      1.555   1.555   1.555

PLAT_732  Alert C Angle   Calc   125.24(4), Rep  125.20(10) ....       2.50 su-Ratio
                     P2   -AG1  -P3      1.555   1.555   1.555

PLAT_732  Alert C Angle   Calc   124.72(4), Rep  124.70(10) ....       2.50 su-Ratio
                     P2   -AG1  -P4      1.555   1.555   1.555

PLAT_732  Alert C Angle   Calc    84.23(3), Rep   84.20(10) ....       3.33 su-Ratio
                     P3   -AG1  -P4      1.555   1.555   1.555


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 8 Alert Level C = Please check

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