Acta Cryst. (2003). E59, m291-m293  [ doi:10.1107/S1600536803008626 ]

A distorted square-planar Pd^II complex with a shortened Pd-Cl bond induced by the bulky terpyridyl ligand 6,6''-dimesityl-2,2':6',2''-terpyridine

A. Onoda, K. Kawakita, T. Okamura, H. Yamamoto and N. Ueyama

Online 30 April 2003

Key indicators

• Single-crystal X-ray study
• T = 200 K
• Mean (C-C) = 0.009 Å
• Disorder in solvent or counterion
• R factor = 0.053
• wR factor = 0.144
• Data-to-parameter ratio = 17.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.48                 
         From the CIF: _reflns_number_total               8029                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         8763                           
         Completeness (_total/calc)             91.62%                          
          Alert C: < 95% complete                                               

PLAT_302  Alert C Anion/Solvent Disorder .......................      21.00 Perc.


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 2 Alert Level C = Please check

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