Acta Cryst. (2003). E59, m399-m401  [ doi:10.1107/S1600536803011772 ]

[(R,R)-1-(N-Benzylideneamino)-2-(diphenylphosphino)cyclohexane-²N,P]dichloro(triphenylphosphine-P)ruthenium(II)

A. Caiazzo, A. J. Lough and A. K. Yudin

Online 10 June 2003

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.011 Å
• R factor = 0.051
• wR factor = 0.118
• Data-to-parameter ratio = 13.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           25.10                 
         From the CIF: _reflns_number_total              12013                  
         Count of symmetry unique reflns         6751                           
         Completeness (_total/calc)            177.94%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured      5262                           
         Fraction of Friedel pairs measured     0.779                           
         Are heavy atom types Z>Si present          yes                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.          

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