Acta Cryst. (2004). E60, i10-i11  [ doi:10.1107/S1600536804000169 ]

Dirubidium tetrathiotungstate, Rb₂[WS₄]

J. Yao and J. A. Ibers

Online 17 January 2004

Key indicators

• Single-crystal X-ray study
• T = 153 K
• Mean (W-S) = 0.001 Å
• R factor = 0.023
• wR factor = 0.061
• Data-to-parameter ratio = 27.3

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low .......       0.94       

Alert level C
REFLT03_ALERT_3_C  Reflection count < 95% complete
           From the CIF: _diffrn_reflns_theta_max           28.89
           From the CIF: _diffrn_reflns_theta_full           0.00
           From the CIF: _reflns_number_total               1119
           TEST2: Reflns within _diffrn_reflns_theta_max
           Count of symmetry unique reflns         1190
           Completeness (_total/calc)             94.03%
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   2 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

Copyright © International Union of Crystallography
IUCr Webmaster