Acta Cryst. (2004). E60, m1334-m1336  [ doi:10.1107/S1600536804020872 ]

Bis[N-(2,6-dimethylphenyl)aminophenylglyoximato-²N,N']nickel(II) dimethyl sulfoxide solvate

H. Bati, A. Zülfikaroglu, M. Tas, N. Çaliskan, S. Soylu, O. Andac and O. Büyükgüngör

Online 31 August 2004

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.003 Å
• Disorder in solvent or counterion
• R factor = 0.037
• wR factor = 0.084
• Data-to-parameter ratio = 13.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT063_ALERT_3_C Crystal Probably too Large for Beam Size .......       0.70 mm    
PLAT243_ALERT_4_C High Solvent U(eq) as Compared to Neighbors  for       C17A     
PLAT244_ALERT_4_C Low  Solvent U(eq) as Compared to Neighbors  for         S1     
PLAT244_ALERT_4_C Low  Solvent U(eq) as Compared to Neighbors  for       C17B     
PLAT301_ALERT_3_C Main Residue  Disorder .........................      22.00 Perc. 
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      43.00 Perc. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   4 ALERT type 4 Improvement, methodology, query or suggestion

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