Acta Cryst. (2004). E60, o1643-o1645  [ doi:10.1107/S1600536804020112 ]

Azidotriphenylsilane: a new determination

I. Wharf and F. Bélanger-Gariépy

Online 31 August 2004

Key indicators

• Single-crystal X-ray study
• T = 220 K
• Mean (C-C) = 0.002 Å
• R factor = 0.039
• wR factor = 0.121
• Data-to-parameter ratio = 14.6

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT241_ALERT_2_B Check High   U(eq) as Compared to Neighbors  for        N32     

Alert level C
PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density ....       2.17       
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors  for        N31     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors  for        N21     
PLAT301_ALERT_3_C Main Residue  Disorder .........................       8.00 Perc. 

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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