Acta Cryst. (2004). E60, m1473-m1474  [ doi:10.1107/S1600536804023086 ]

Dichloro{1-[2-(diphenylphosphino-P)ethyl]-1,3-dihydro-3-(2,4,6-trimethylphenyl)-2H-imidazol-2-ylidene-C}palladium(II) diethyl ether solvate

H. M. Lee and P. L. Chiu

Online 25 September 2004

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.005 Å
• R factor = 0.031
• wR factor = 0.080
• Data-to-parameter ratio = 20.3

checkCIF/PLATON results

No syntax errors found



Alert level A
DIFF020_ALERT_1_A  _diffrn_standards_interval_count and
            _diffrn_standards_interval_time are missing. Number of measurements
            between standards or time (min) between standards.
DIFF022_ALERT_1_A  _diffrn_standards_decay_% is missing
            Percentage decrease in standards intensity.

Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.82 Ratio 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H2A    ..  CL2     ..       2.93 Ang.  
PLAT480_ALERT_4_C Long H...A H-Bond Reported H5A    ..  CL1     ..       2.90 Ang.  

   2 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   3 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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