Acta Cryst. (2005). E61, m778-m780  [ doi:10.1107/S1600536805008913 ]

Chlorobis[2-(2-pyridyl)phenyl-²N,C¹](triphenylphosphine-P)iridium(III) dichloromethane sesquisolvate

Y. Wang, F. Teng, A. Tang, Y. Wang and X. Xu

Online 31 March 2005

Key indicators

• Single-crystal X-ray study
• T = 193 K
• Mean (C-C) = 0.013 Å
• Disorder in solvent or counterion
• R factor = 0.051
• wR factor = 0.120
• Data-to-parameter ratio = 14.7

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings    Differ ....          ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............       0.50 Ratio 
PLAT202_ALERT_3_C Isotropic non-H Atoms in Anion/Solvent .........          1       
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        C41     
PLAT302_ALERT_4_C Anion/Solvent Disorder .........................      14.00 Perc. 
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         12       

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   7 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   0 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion

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