Acta Cryst. (2005). E61, m1343-m1345  [ doi:10.1107/S1600536805018246 ]

Poly[(₃-n-hexane-1,6-dicarboxylato)dysprosium(III)]

D. T. Lill, W. W. Brennessel, L. A. Borkowski, N. S. Gunning and C. L. Cahill

Online 17 June 2005

Key indicators

• Single-crystal X-ray study
• T = 173 K
• Mean (C-C) = 0.007 Å
• Disorder in main residue
• R factor = 0.029
• wR factor = 0.079
• Data-to-parameter ratio = 18.5

checkCIF/PLATON results

No syntax errors found




Alert level B
REFLT01_ALERT_1_B  The number of symmetry-independent reflections cannot
            exceed the total number of reflections measured
            Number of symmetry-independent reflections =   3139
            Total number of reflections                =   3106

Alert level C
PLAT030_ALERT_1_C _diffrn_reflns_number .LE.  _reflns_number_total          ?
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT301_ALERT_3_C Main Residue  Disorder .........................       9.00 Perc. 
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .      40.00 A   3  
PLAT764_ALERT_4_C Overcomplete CIF Bond List Detected (Rep/Expd) .       1.12 Ratio 

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion

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