Acta Cryst. (2006). E62, m2916-m2918  [ doi:10.1107/S1600536806041146 ]

(-Diphenylphosphido-P:P)--hydrido-(-4-hydroxybenzenethiolato-²S:S)bis[(⁶-hexamethylbenzene)ruthenium(II)] tetrafluoroborate

M.J.-L. Tschan, F. Chérioux, B. Therrien, L. Karmazin-Brelot and G. Süss-Fink

Online 13 October 2006

Key indicators

• Single-crystal X-ray study
• T = 173 K
• Mean (C-C) = 0.005 Å
• R factor = 0.032
• wR factor = 0.062
• Data-to-parameter ratio = 15.8

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.81 Ratio
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for         B1     
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety        C31     
PLAT380_ALERT_4_C Check Incorrectly? Oriented X(sp2)-Methyl Moiety        C35     
PLAT412_ALERT_2_C Short Intra XH3 .. XHn     H22C   ..  H23B    ..       1.86 Ang. 
PLAT412_ALERT_2_C Short Intra XH3 .. XHn     H33C   ..  H34A    ..       1.86 Ang. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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