Acta Cryst. (2006). E62, m3511-m3513  [ doi:10.1107/S1600536806050318 ]

Di--iodo-tris(tri-p-tolylphosphine)-1P,2²P-dicopper(I)

R. Meijboom

Online 30 November 2006

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.007 Å
• R factor = 0.045
• wR factor = 0.101
• Data-to-parameter ratio = 20.9

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  I1     -   Cu1     ..      16.54 su   
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  I1     -   Cu2     ..      21.38 su   
PLAT232_ALERT_2_B Hirshfeld Test Diff (M-X)  I2     -   Cu2     ..      11.40 su   

Alert level C
PLAT154_ALERT_1_C The su's on the Cell Angles are Equal (x 10000)        3000 Deg. 
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.41 Ratio
PLAT222_ALERT_3_C Large Non-Solvent    H     Ueq(max)/Ueq(min) ...       3.80 Ratio
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  I2     -   Cu1     ..       5.22 su   
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for         I2     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C22     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C25     
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C65     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C14     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C21     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C24     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C44     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C61     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C64     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C84     

Alert level G
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature .        293 K    

   0 ALERT level A = In general: serious problem
   3 ALERT level B = Potentially serious problem
  15 ALERT level C = Check and explain
   2 ALERT level G = General alerts; check

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  16 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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