Acta Cryst. (2006). E62, m3163-m3164  [ doi:10.1107/S1600536806044771 ]

{6,6'-Dimethoxy-2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}(ethanol)dioxouranium(VI)

N. Senyüz, Ç. Yüksektepe, H. Bati, N. Çaliskan and O. Büyükgüngör

Online 3 November 2006

Key indicators

• Single-crystal X-ray study
• T = 296 K
• Mean (C-C) = 0.016 Å
• R factor = 0.042
• wR factor = 0.099
• Data-to-parameter ratio = 15.4

checkCIF/PLATON results

No syntax errors found






Alert level C
RINTA01_ALERT_3_C  The value of Rint is greater than 0.10
            Rint given   0.104
PLAT020_ALERT_3_C The value of Rint is greater than 0.10 .........       0.10      
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       3.35 Ratio
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C17     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for         O5     
PLAT342_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         16      

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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