Acta Cryst. (2006). E62, m3429-m3431  [ doi:10.1107/S1600536806048604 ]

Aquachlorobis(1,10-phenanthroline)nickel(II) chloride thioacetamide solvate

H. Zhong, X.-R. Zeng and Q.-Y. Luo

Online 24 November 2006

Key indicators

• Single-crystal X-ray study
• T = 273 K
• Mean (C-C) = 0.008 Å
• R factor = 0.043
• wR factor = 0.126
• Data-to-parameter ratio = 16.0

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low .......       0.97      
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT244_ALERT_4_C Low   'Solvent' Ueq as Compared to Neighbors for        C25     
PLAT341_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...          8      
PLAT362_ALERT_2_C Short  C(sp3)-C(sp2) Bond  C25    -   C26    ...       1.38 Ang. 
PLAT480_ALERT_4_C Long H...A H-Bond Reported H24    ..  CL1     ..       2.86 Ang. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   2 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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