Acta Cryst. (2006). E62, m3496-m3497  [ doi:10.1107/S1600536806049543 ]

Di--chloro-bis({3-[(2-hydroxy-1-methyl-2-phenylethyl)iminomethyl]-2-naphtholato-³N,O,O'}copper(II)) methanol solvate

S.-A. Li, Y.-C. Jin, T.-T. Xu, D.-Q. Wang and J. Gao

Online 30 November 2006

Key indicators

• Single-crystal X-ray study
• T = 298 K
• Mean (C-C) = 0.013 Å
• R factor = 0.066
• wR factor = 0.211
• Data-to-parameter ratio = 14.2

checkCIF/PLATON results

No syntax errors found




Alert level C
RINTA01_ALERT_3_C  The value of Rint is greater than 0.10
            Rint given   0.118
PLAT020_ALERT_3_C The value of Rint is greater than 0.10 .........       0.12      
PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low ....         48 Perc.
PLAT220_ALERT_2_C Large Non-Solvent    C     Ueq(max)/Ueq(min) ...       2.65 Ratio
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Cu1    -   Cl2     ..       7.04 su   
PLAT341_ALERT_3_C Low Bond Precision on C-C bonds (x 1000) Ang ...         13      
PLAT410_ALERT_2_C Short Intra H...H Contact  H1     ..  H10     ..       1.99 Ang. 
PLAT410_ALERT_2_C Short Intra H...H Contact  H21    ..  H30     ..       1.97 Ang. 

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   8 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   4 ALERT type 2 Indicator that the structure model may be wrong or deficient
   4 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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