Acta Cryst. (2008). E64, m755  [ doi:10.1107/S1600536808011975 ]

Bis[1,5-bis(1H-indol-3-ylmethylene)thiocarbazonato-²N,S]nickel(II) dimethyl sulfoxide disolvate

M. R. Rizal, H. M. Ali and S. W. Ng

Online 3 May 2008

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.005 Å
• R factor = 0.049
• wR factor = 0.139
• Data-to-parameter ratio = 18.2

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT420_ALERT_2_C D-H Without Acceptor       N3     -   H3N    ...          ?      

Alert level G
FORMU01_ALERT_1_G  There is a discrepancy between the atom counts in the
            _chemical_formula_sum and _chemical_formula_moiety. This is
            usually due to the moiety formula being in the wrong format.
            Atom count from _chemical_formula_sum:   C42 H42 N12 Ni1 O2 S4
            Atom count from _chemical_formula_moiety:C4 H12 O2 S2

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   2 ALERT level C = Check and explain
   1 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   0 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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