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Acta Cryst. (2010). E66, m314  [ doi:10.1107/S1600536810005933 ]

catena-Poly[[tris(4-fluorobenzyl)tin(IV)]{[mu]-[(N,N-diisopropylcarbamothioyl)sulfanyl]acetato-[kappa]2O:O'}]

T. C. Keng, K. M. Lo and S. W. Ng

Online 20 February 2010


Key indicators

checkCIF/PLATON results

No syntax errors found




Alert level B PLAT601_ALERT_2_B Structure Contains Solvent Accessible VOIDS of . 142.00 A   3
Author Response: SEE Experimental

PLAT919_ALERT_3_B Reflection(s) # Likely Affected by the Beamstop           2      

Alert level C PLAT029_ALERT_3_C _diffrn_measured_fraction_theta_full Low ....... 0.97 PLAT222_ALERT_3_C Large Non-Solvent H Ueq(max)/Ueq(min) ... 3.31 Ratio PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C5 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C25 PLAT342_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang .. 10 PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 30 PLAT972_ALERT_2_C Large Calcd. Non-Metal Negative Residual Density -1.59 eA-3 PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L= 0.600 212
Alert level G PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature 293 K PLAT200_ALERT_1_G Check the Reported _diffrn_ambient_temperature 293 K
0 ALERT level A = In general: serious problem 2 ALERT level B = Potentially serious problem 8 ALERT level C = Check and explain 2 ALERT level G = General alerts; check 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 4 ALERT type 2 Indicator that the structure model may be wrong or deficient 5 ALERT type 3 Indicator that the structure quality may be low 1 ALERT type 4 Improvement, methodology, query or suggestion 0 ALERT type 5 Informative message, check

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