Acta Cryst. (2010). E66, m481  [ doi:10.1107/S1600536810011372 ]

(4-Methylbenzohydrazidato-²N',O)[2-(4-methylbenzoylhydrazinylidene-²N,O)-3-phenylpropionato(2-)]oxidovanadium(V) methanol monosolvate

H. W. Wong, K. M. Lo and S. W. Ng

Online 31 March 2010

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.006 Å
• R factor = 0.054
• wR factor = 0.167
• Data-to-parameter ratio = 17.7

checkCIF/PLATON results

No syntax errors found




Alert level C
PLAT241_ALERT_2_C Check High      Ueq as Compared to Neighbors for        C22     
PLAT242_ALERT_2_C Check Low       Ueq as Compared to Neighbors for        C20     
PLAT432_ALERT_2_C Short Inter X...Y Contact  C26    ..  C26     ..       3.14 Ang. 
PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L=  0.600          3      
PLAT731_ALERT_1_C Bond    Calc   1.426(10), Rep    1.426(4) ......       2.50 su-Ra
              O6   -C26     1.555   1.555                                      
PLAT912_ALERT_4_C Missing # of FCF Reflections Above STh/L=  0.600         15      

Alert level G
PLAT860_ALERT_3_G Note: Number of Least-Squares Restraints .......         13      
PLAT154_ALERT_1_G The su's on the Cell Angles are Equal  (x 10000)        200 Deg. 
PLAT199_ALERT_1_G Check the Reported _cell_measurement_temperature        293 K    
PLAT200_ALERT_1_G Check the Reported   _diffrn_ambient_temperature        293 K    

   0 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   6 ALERT level C = Check and explain
   4 ALERT level G = General alerts; check

   4 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   1 ALERT type 4 Improvement, methodology, query or suggestion
   0 ALERT type 5 Informative message, check

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